Application of 7170-01-6, A common heterocyclic compound, 7170-01-6, name is 3-Methyl-1H-1,2,4-triazole, molecular formula is C3H5N3, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
A mixture of Zn(NO3)2.6H2O (30.0 mg, 0.1 mmol), 3-amino-1,2,4-triazole (8.4 mg, 0.1 mmol), H2bdc (8.3 mg, 0.05 mmol) and HNO3 (0.08 mL) in a mixed solvents of DMA (1.5 mL), MeOH(1.5 mL) and H2O (3 mL) was placed in a glass vial (23 mL) and heated at 100 C for 3 days. Colorless polyhedral crystals were obtained and washed with MeOH (yield: 75% based on ligand).Anal. Calc. (Found) for C12H11Zn2N8O4.5: C, 30.66 (30.62); H, 2.36(2.26); N, 23.84 (23.82)%. Selected IR data (KBr, cm-1): 3413,3337, 3231, 1633, 1588, 1541, 1390, 1404, 1290, 1227, 1067,1013, 885, 830, 746, 583.
The synthetic route of 7170-01-6 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Liu, Jie; Wei, Yuhui; Bao, Fenlin; Li, Guixiang; Liu, Huiyan; Wang, Haiying; Polyhedron; vol. 169; (2019); p. 58 – 65;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics