Related Products of 584-13-4, These common heterocyclic compound, 584-13-4, name is 4H-1,2,4-Triazol-4-amine, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Add 0.033 mol of 4-amino-1,2,4-triazole to 60 mL of water.0.035 mol sodium carbonate, stirred for 10 min in an ice bath,Cyanuric chloride solution was added dropwise in 10 min,Stir at 100 C for 10 hours, cool to room temperature, and filter by suction.Washing three times with water at 5 C, drying at 70 C, to obtain a s-triazine-based fluorescent probe, yield 95%;The cyanuric chloride solution,Are 0.01 mol of cyanuric chloride in 30 mL of 1,4-dioxane mixed solution was obtained.
The synthetic route of 584-13-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; University of Jinan; Wang Zhiling; Kuang Xuan; Cui Yu; Sun Xu; Zhang Yong; (7 pag.)CN108047210; (2018); A;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics